Process for the preparation of coated granular sodium...

Chemistry of inorganic compounds – Carbon or compound thereof – Oxygen containing

Reexamination Certificate

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Details

C423S415100, C423S421000, C423S275000, C252S186270, C252S186320, C510S444000, C510S446000, C510S456000, C427S213000, C427S215000, C427S314000

Reexamination Certificate

active

10223351

ABSTRACT:
The invention relates to a process for the preparation of coated granular sodium percarbonate having a low TAM value. The preparation is carried out by fluidized-bed spray granulation at a temperature TGin the range from 45 to 75° C., and the coating is effected by the spray application of an aqueous solution containing at least one coating component in a fluidized bed at a temperature TUin the range from 35 to 100° C. According to the invention, a) after the fluidized-bed spray granulation but before the coating, drying is carried out at TNTof greater than TG, or b) the fluidized-bed granulation is carried out in at least two steps at TG1, TG2. . . TGn, TG2or TGnbeing higher than TG1, and drying being unnecessary if ⅔ of the granulate have been formed at TG1, or c) drying takes place not after the granulation but after the coating, at TUNT, TUNTbeing at least 20° C. higher than TG.

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