Process for the preparation of an acetamide derivative

Details Process for the preparation of an acetamide derivative Process for the preparation of an acetamide derivative

1977-05-25

1978-11-28

Demers, Arthur P.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C103127

Patent

active

041276078

ABSTRACT:
Process for preparing di-n-propyl acetamide of the formula: ##STR1## whereby di-n-propyl acetonitrile is hydrolyzed by means of 80% sulphuric acid aqueous solution in the proportion of 2 to 2.5 g of dilute acid/g of nitrile, at a temperature between 80.degree. C and 130.degree. C to obtain the desired amide.

REFERENCES:
Keil, Z. Physiol Chem. 282 (1947), pp. 137-142.
Hessler et al., J. Am. Chem. Soc. 43, pp. 205-207.
Sarel et al., J. Am. Chem. Soc. 78, pp. 5416-5420.
Sperber et al., J. Am. Chem. Soc. 70, pp. 3091-3094.
Tsai et al., J. Am. Chem. Soc. 70, pp. 2530-2533.

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