Process for the preparation of alkylthioacetamidines

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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C07C12300

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047134909

ABSTRACT:
A process for the preparation of alkylthioacetamidines by the reaction of chloroacetonitrile with ammonium halide in the presence of a catalyst followed by reaction of the resultant chloroacetamidine with an alkyl mercaptan in the presence of an acid acceptor.

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Degering, Ed. F. An Outline of Organic Nitrogen Compounds, (1950), Univ. Lithoprinters, Ypsilanti, Mich., Publ. at p. 506.
Kirk-Othmer, Encyclopedia of Chemical Technology, 2nd Ed., (1970), vol. 20, at p. 211.
Conant, James Bryant et al., The Chemistry of Organic Compounds, 45h Ed., (1954), MacMillan Co., Publ. pp. 335-338.
Quayle, Osborne R., J. Am. Chem. Society., (1942), vol. 64, pp. 226-230.

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