Process for the preparation of alkyl methyl-3-carbalkoxyethylpho

Details Process for the preparation of alkyl methyl-3-carbalkoxyethylpho Process for the preparation of alkyl methyl-3-carbalkoxyethylpho

1990-10-18

1992-10-06

Lee, Mary C.

Organic compounds -- part of the class 532-570 series

Organic compounds

Phosphorus esters

558179, C07F 940

Patent

active

051533456

ABSTRACT:
Process for the preparation of compounds of the formula ##STR1## where R is (C.sub.1 -C.sub.4)alkyl, which comprises reacting a compound of the formula II ##STR2## with an alcoholate of the formula III

REFERENCES:
patent: 4062888 (1977-12-01), Ohorodnik et al.
patent: 4399287 (1983-08-01), Baillie et al.
Houben-Weyl, Methoden der Organischen Chemie, Bd. XII/1, p. 248 (1963).
Khairullin, et al., Reaction of Methyldichlorophosphine with Acrylic Acid, Translated from Zhurnal Obshchei Khimii, vol. 37, No. 3, pp. 710-714 (1967).
Khairullin, et al., Synthesis and Some Properties of Ethyl 3-(chloroethylphosphinyl) propionate, Translated from Zhurnal Obshchei Khimii, vol. 39, No. 2, pp. 341-346 (1969).
Khairullin, V. K., Reaction of Ethyldichlorophosphine with .alpha., .beta.-unsaturated acids, Translated from Doklady Akademii Nauk SSSR, vol. 162, No. 4, pp. 827-828 (1965).
Khairullin, et al., Reaction of Ethylphosphonous Dichloride with Crotonic Acid, Translated from Zhurnal Oshchei Khimii, vol. 36, No. 3, pp. 494-498 (1966).
March, J. Advanced Organic Chemistry, Third Edition, J. Wiley and Sons, 1985, pp. 346-347.
Wagner et al. "Synthetic Organic Chemistry", (1953) pp. 481-482.

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