Process for the preparation of a graphite intercalation compound

Details Process for the preparation of a graphite intercalation compound Process for the preparation of a graphite intercalation compound

1986-08-05

1988-03-08

Heller, Gregory A.

Chemistry of inorganic compounds

Carbon or compound thereof

Elemental carbon

423445, 423449, 423460, 252502, 252506, 252508, H01B 106

Patent

active

047298847

ABSTRACT:
In the production of a graphite intercalation compound in which the intercalant is a metal chloride, the reaction is carried out in the presence of a second metal chloride of a relatively low boiling point to effect a notable reduction in the reaction time. In the production of a metal chloride intercalation compound which normally requires an atmosphere of chlorine, the addition of the second metal chloride permits the reaction to proceed in the absence of chlorine gas.

REFERENCES:
patent: 3956194 (1976-05-01), Armand
patent: 4560409 (1985-12-01), Goldberger et al.
patent: 4565649 (1986-01-01), Vogel
patent: 4604276 (1986-08-01), Oblas et al.
patent: 4608192 (1986-08-01), Su
Y. Iye et al, Phys. Rev. B, 25, 4583, 1982.
F. Vogel et al., Bull. Am. Phys. Soc., 21, 262, 1976.
Takahashi et al., Glossary of Lectures for the 11th Annual Meeting of the Carbon Society of Japan, p. 42, 1984.
S. Flandrois, Synth. Met., 3, 1, 1981.
E. Stumpp, Mat. Sci. Eng., 31, 53, 1977.

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