Process for the preparation of 8,14-cedranoxide

Details Process for the preparation of 8,14-cedranoxide Process for the preparation of 8,14-cedranoxide

1972-08-22

1976-06-01

Randolph, John D.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

204158R, 260343, 260563P, 2606315, C07D30700

Patent

active

039608999

ABSTRACT:
Processes for the preparation of 8,14-cedranoxide are disclosed, according to which 8,14-cedrane diol is prepared by reducing 8,14-cedranolide by treatment with the aid of diisobutyl-aluminum hydride followed by acid hydrolysis, or 8,14-cedrane diol is cyclized with dimethyl sulfoxide.

REFERENCES:
patent: 3522276 (1970-07-01), Gibson
Baggaley et al., Tetrahedron (1968) vol. 24, pp. 3399-3405.
Fieser et al., Reagents for Organic Synthesis, New York, John Wiley (1966) pp. 261, 262, 301-302, and 586.
Barton et al., J. Am. Chem. Soc. (1960) vol. 82, pp. 2640-2641.

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