Process for the preparation of 3-trichloromethyl-5-chloro-1,2,4-

Details Process for the preparation of 3-trichloromethyl-5-chloro-1,2,4- Process for the preparation of 3-trichloromethyl-5-chloro-1,2,4-

1975-03-31

1976-09-07

Rizzo, Nicholas S.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260453R, C07D28508

Patent

active

039794032

ABSTRACT:
A process is provided for preparing 3-trichloromethyl-5-chloro-1,2,4-thiadiazole in improved yields by reacting a defined molar excess trichloroacetamidine with trichloromethanesulfenyl chloride while controlling pH of the reaction mixture. The present process may advantageously be employed in a batch or continuous process.

REFERENCES:
patent: 3260725 (1966-07-01), Schroeder

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