Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh

Details Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh

1990-09-20

1992-08-25

Brust, Joseph Paul

Organic compounds -- part of the class 532-570 series

Organic compounds

Nitriles

558421, C07C25310

Patent

active

051420902

ABSTRACT:
The present invention relates to a process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cyclohexanone by means of the reaction of isophorone with an alkaline cyanide. The reaction is performed starting from isophorone and an equivalent amount of cyanide in a homogeneous water/organic solvent solution at a temperature comprised between 20.degree. C. and the reflux temperature, maintaining a pH between 14 and 8 by means of a gradual addition of an inorganic acid during the reaction.

REFERENCES:
patent: 3352913 (1967-11-01), Schmitt et al.
patent: 4299775 (1981-11-01), Dubreux
Lange, "Manuale Di Chimica", (date not available), pp. 368-369; Uses Utet-Sansoni Edizioni Scientifiche Firenze.
Kuster-Thiel, Tabelle Per Le Analisi Chimidre E Chimico-Fisiche, 12th ed, (date not available), p. 138, Ulrico Hoepli Editore Milano.

Affiliated with

Also associated with

Rating

Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the preparation of 3-cyano-3,5,5'-trimethyl-1-cycloh will most certainly appreciate the feedback.

Rate now

Comments { 0 }

Profile ID: LFUS-PAI-O-386396