Process for the preparation of 2,4-dinitroaniline

Details Process for the preparation of 2,4-dinitroaniline Process for the preparation of 2,4-dinitroaniline

1976-08-10

1978-07-25

Douglas, Winston A.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07C 8504

Patent

active

041029275

ABSTRACT:
2,4-DINITROANILINE IS OBTAINED IN HIGH YIELD AND QUALITY IN A SAFE REACTION BY INTRODUCING 4-CHLORO-1,3-DINITROBENZENE INTO AT LEAST THREE-FOLD STOICHIOMETRIC AMOUNT OF AQUEOUS AMMONIA OF A CONCENTRATION OF 15 TO 40% BY WEIGHT AT A TEMPERATURE OF 60.degree. TO 90.degree. C.

REFERENCES:
sidgwick, "The Organic Chemistry of Nitrogen", p. 143, (1966).

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