Process for the preparation of 1-hydroxylated vitamin D compound

Details Process for the preparation of 1-hydroxylated vitamin D compound Process for the preparation of 1-hydroxylated vitamin D compound

1979-11-06

1981-04-21

Roberts, Elbert L.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

C07J 900

Patent

active

042632153

ABSTRACT:
1-Hydroxy-5,6-trans vitamin D compounds are prepared by oxidizing a 5,6-trans vitamin D compound using a selenic ester which may be formed in situ using selenous acid or selenium dioxide in the presence of an alcohol.

REFERENCES:
patent: WO79/00513 (1979-08-01), De Luca et al.
"Steroids", published Aug. 1977, vol. 30, No. 2, pp. 193-201, by Pelc et al.

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