Process for the manufacture of the gamma-crystal modification of

Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...

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106288Q, C09B 4800

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active

042129753

ABSTRACT:
Unsubstituted linear trans-quinacridone of the gamma-crystal modification is obtained by cyclization of 2,5-dianilino-terephthalic acid with the 2.5 to 4-fold quantity of polyphosphoric acid or of an acidic polyphosphoric acid methyl ester, followed by hydrolysis of the condensation product in water, intensive grinding of the aqueous crude quinacridone in the presence of an alcohol or ketone and heating of the resulting product to 80.degree. to 200.degree. C.

REFERENCES:
patent: 3257405 (1966-06-01), Gerson et al.
patent: 3265699 (1966-08-01), Jaffe
patent: 4100162 (1978-07-01), North

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