Process for the manufacture of polyuronic acids

Organic compounds -- part of the class 532-570 series – Organic compounds – Carbohydrates or derivatives

Reexamination Certificate

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

Reexamination Certificate

active

06903209

ABSTRACT:
Disclosed is a polyuronic acid having an average degree of polymerization less than 20. The method of the present invention comprises the steps: (a) providing a solution containing 5 wt. % or more of a high molecular weight polyuronic acid predominantly as its lithium salt; (b) adding hydrogen peroxide and a ferrous salt to the solution prepared in step (a) to oxidatively degrade the high molecular weight polyuronic acid; and (c) isolating a polyuronic acid having an average degree of polymerization less than 20 obtained in step (b).

REFERENCES:
patent: 244249 (1997-03-01), None
patent: 0487340 (1992-05-01), None
patent: 1250516 (1971-10-01), None
Natsume, M., et al. “Isolation and characterization of alginate-derived oligosaccharides with root growth-promoting activities” Carbohydrate Research, vol. 258, p. 187-197, (1994).
Yonemoto, Y., et al. “Promotion of Germination and Shoot Elongation of Some Plants by Alginate Oligomers . . . Lyase” Journal of Fermentation and Bioengineering, vol. 75, No. 1, p. 68-70, (1993).
Haug, A., et al. “Studies on the Sequence of Uronic Acid Residues in Alginic Acid” Acta Chemica Scandinavica, vol. 21, p. 691-704, (1967).
Haug, A., et al. “Development of Compositional Heterogeneity in Alginate Degraded in Homogeneous Solution” Acta Chemica Scandinavica, vol. 23, p. 2955-2962, (1969).
O'Colla, P.S., et al. “The Action of Fenton's Reagent on Acidic Polysaccharides” Proc. Chem. Soc., p. 68-69, (1962).
Smidsrod, O., et al. “Kinetic Studies on the Degradation of Alginic Acid by Hydrogen Peroxide in the Presence of Iron Salts” Acta Chemica Scandinavica, vol. 19, p. 143-152, (1965).
Baxendale, J.H. “Decomposition of Hydrogen Peroxide by Catalysts in Homogeneous . . . Solution” Advances in Catalysis and Related Subjects, vol. IV, Eds. Frankenburg, W.G., et al. p. 31-86, (1952).
Smidsrod, O., et al. “Degradation of Alginate in the Presence of Reducing Compounds” Acta Chemica Scandinavica, vol. 17, p. 2628-2637, (1963).
Kumazawa, Y., et al., “Immunostimulating polysaccharide separated from hot water extract ofAngelica acutilobaKitagawa (Yamato Tohki)” Immunology, vol. 47, p. 75-83, (1982).
Nothnagel, E.A., et al. “Host-Pathogen Interactions: XXII. A Galacturonic Acid Oligosaccharide from Plant Cell Walls Elicits Phytoalexins” Plant Physiol., vol. 71, p. 916-926, (1983).
Kohn, R., et al. “The Activity of Calcium Ions in Aqueous Solutions of the Lower Calcium Oligogalacturonates” Carbohydrate Research, vol. 20, p. 351-356, (1971).
Liu, Y.K., et al. “Quantitative Aspects of Pectic Acid Hydrolysis by Endo-Polygalacturonase fromRhizopus Arrhizus” Journal of food Science, vol. 45, p. 601-604, (1980).
von Euler, V.H., et al. “Oxydative Decarboxylierung des Pektins, derDiketogulonsaure (Dehydro-ascorbinsaure) und der Brenztraubensaure”, Makromol. Chem, vol. 18/19, p. 375-382, (1956).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Process for the manufacture of polyuronic acids does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for the manufacture of polyuronic acids, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for the manufacture of polyuronic acids will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-3487754

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.