Process for the manufacture of hydroxylammonium perchlorate

Chemistry of inorganic compounds – Halogen or compound thereof – Ternary compound

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C01B 1116

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043350917

ABSTRACT:
Hydroxylammonium perchlorate is obtained by reacting a perchlorate-free hydroxylammonium salt with a perchlorate ions-donating compound, the reaction being carried out in aqueous solution with the aid of a cation exchanger, in parallel flow or preferably in countercurrent direction. The hydroxylammonium perchlorate is obtained in a high yield and in a high purity. It is suitable as oxidant in fuels.

REFERENCES:
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patent: 3928546 (1975-12-01), Guzzo
patent: 4066736 (1978-01-01), Liggett
Schumacher et al., "Large-Scale Continuous Production of Ammonium Perchlorate", Chemical Engineering Progress, Sep. 1957, (vol. 53, No. 9, pp. 428-432.

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