Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material
Patent
1981-01-09
1982-09-14
Bascomb, Jr., Wilbur L.
Distillation: processes, separatory
With chemical reaction
Including step of adding catalyst or reacting material
203 36, 203 37, 203 38, 203 71, 568867, 568868, B01D 334, C07C 2980, C07C 3120
Patent
active
043494170
ABSTRACT:
Ethylene oxide and water are reacted in a reactor and the reaction product is subjected to distillation in a plurality of distillation columns, in the first columns water and components having a boiling point below that of monoethylene glycol and higher ethylene glycols, if any, being distilled off. To obtain extremely pure monoethylene glycol alkali metal compounds are added at a point between the reactor and the monoethylene glycol distillation column in an amount to adjust the pH of the product entering the latter column to a value of from 7 to 10. The monoethylene glycol obtained in this manner is especially pure and has very low UV absorption values. It is, therefore, especially suitable for the manufacture of polyester fibers.
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patent: 2788373 (1957-04-01), Mills et al.
patent: 2793235 (1957-05-01), Jenkinson
patent: 3408268 (1968-10-01), Pitts et al.
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patent: 3904656 (1975-09-01), Broz
patent: 3970711 (1976-07-01), Reiche et al.
patent: 4225394 (1980-09-01), Cox et al.
Alfranseder Josef
Mayer Sigmund
Rebsdat Siegfried
Schaffelhofer Iwo
Bascomb, Jr. Wilbur L.
Hoechst Aktiengesellschaft
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