Process for the manufacture of dialkyl disulfides

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfur containing

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568 71, C07C31924

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active

050269151

ABSTRACT:
A continuous process is disclosed for preparing dialkyl disulfides by reacting an alkyl alcohol and hydrogen sulfide in one reaction zone, and then passing the reactor effluent into a second reaction zone where it is reacted with elemental sulfur in the presence of a solid, particulate catalyst.

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K. Liu, Synthesis, Sep. '78, (9) pp. 669-670, "A Facile Conversion of Thiols to Disulfides".
E. E. Reid, "Organic Chemistry of Bivalent Sulfur", vol. 1, pp. 118-126 (1958).

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