Process for the manufacture of 6-methyl-3,4-dihydro-1,2,3-oxathi

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07D29106

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039681076

ABSTRACT:
6-Methyl-3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide and the nontoxic salts thereof are prepared by reacting acetoacetic acid with fluorosulfonyl isocyanate at a temperature of from -20.degree.C to +50.degree.C in the presence of from 0.5 to 2 moles, calculated on the FSI used, of an alkali methal fluoride or a tertiary amine of the formula

REFERENCES:
patent: 3917589 (1975-11-01), Clauss et al.

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