Process for the isolation of .beta.-sitosterol containing a low

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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C07J 900

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042658241

ABSTRACT:
A process for the isolation and recovery of .beta.-sitosterol substantially free of .alpha.-sitosterol from the unsaponifiables obtained from crude soap skimmings or from a crude sterol mixture containing .beta.-sitosterol, .alpha.-sitosterol and campesterol. The starting material is treated with an inorganic or organic acid in an organic solvent, whereby .alpha.-sitosterol reacts with the acid giving rearrangement products. The solution is cooled and filtered or the solvent is distilled off, whereafter the obtained crude .beta.-sitosterol is recrystallized from an organic solvent, to yield the pure material.

REFERENCES:
patent: 2322906 (1943-06-01), Yoder
patent: 2573265 (1951-10-01), Lange et al.
patent: 4153622 (1979-05-01), Lamminkari et al.

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