Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1979-12-05
1981-05-05
Roberts, Elbert L.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07J 900
Patent
active
042658241
ABSTRACT:
A process for the isolation and recovery of .beta.-sitosterol substantially free of .alpha.-sitosterol from the unsaponifiables obtained from crude soap skimmings or from a crude sterol mixture containing .beta.-sitosterol, .alpha.-sitosterol and campesterol. The starting material is treated with an inorganic or organic acid in an organic solvent, whereby .alpha.-sitosterol reacts with the acid giving rearrangement products. The solution is cooled and filtered or the solvent is distilled off, whereafter the obtained crude .beta.-sitosterol is recrystallized from an organic solvent, to yield the pure material.
REFERENCES:
patent: 2322906 (1943-06-01), Yoder
patent: 2573265 (1951-10-01), Lange et al.
patent: 4153622 (1979-05-01), Lamminkari et al.
Koskenniska Lasse A.
Puhakka Marie M.
Farmos-yhtyma Oy
Roberts Elbert L.
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