Process for the hydroperoxidation of branched alkanes in a plura

Details Process for the hydroperoxidation of branched alkanes in a plura Process for the hydroperoxidation of branched alkanes in a plura

1975-07-02

1977-01-11

Thomas, Jr., James O.

Chemistry of carbon compounds

Miscellaneous organic carbon compounds

C-metal

260610A, C07C17902

Patent

active

040026876

ABSTRACT:
Process, and resulting product, for improved hydroperoxidation of branched alkanes of at least 4 carbon atoms, especially useful in preparation of isoprene from isopentane; comprising the substantial elimination of acetic acid and similar by-products in the hydroperoxidation reaction which are harmful to the yield of the desired hydroperoxides; all of which is achieved by at least one washing between at least two successive oxidizing reactors. The wash solution may be just water or advantageously a pre-saturated aqueous solution containing the oxidation products which are desired not to be extracted from the organic phase of the reaction medium.

REFERENCES:
patent: 2825742 (1958-03-01), Schueler et al.
patent: 2862973 (1958-12-01), Winkler et al.

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