Process for the cyclization of orthobenzoylbenzoic acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Polycyclo ring system containing anthracene configured ring...

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C07C 5018

Patent

active

049669842

ABSTRACT:
The process for the cyclization of orthobenzoylbenzoic acid into anthraquinone comprising heating orthobenzoylbenzoic acid in the solid phase at a temperature between about 300.degree. C. to 400.degree. C. in the presence of a superactive bleaching earth. The invention also comprises a process for the separation of phthalic acid and any phthalic anhydride impurities from orthobenzoylbenzoic acid prior to its cyclization into anthraquinone through the use of said earth at a temperature from 200.degree. C. to 250.degree. C.

REFERENCES:
patent: 4045456 (1977-08-01), Merger et al.

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