Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1989-03-14
1990-12-11
Lone, Werren B.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
2604106, 560224, 560234, C11C 302
Patent
active
049768921
ABSTRACT:
A process for the continuous transesterification of C.sub.6 -C.sub.22 fatty acid lower alkyl esters, particularly methyl esters, with polyhydric C.sub.2 -C.sub.5 alcohols, particularly glycerol, in a reaction column comprising a rectifying and reaction section, alkaline catalysts and polyhydric alcohol are introduced into the upper part of the reaction column and boiling fatty acid methyl ester is introduced into the middle part of the reaction column. The product collected in the sump of the column is removed, heated and returned to the lower part of the reaction column. Product is removed from the sump. Lower alkanols passing from the reaction column section to the rectifying section are rectified. The reaction column is operated in boiling equilibrium in its lower part and predominantly in an absorption/desorption equilibrium in its upper part.
REFERENCES:
patent: 4381407 (1983-04-01), Bremus et al.
JOACS, 59, No. 10, 795A-802A, Oct. 1982.
Gutsche Bernhard
Jeromin Lutz
Peukert Eberhard
Schleper Bernard
Wollmann Gerhard
Clarke Vera C.
Henkel Kommanditgesellschaft auf Aktien
Jaeschke Wayne C.
Lone Werren B.
Ortiz Daniel S.
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