Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1975-05-30
1977-04-12
Milestone, Norma S.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07D30128
Patent
active
040175235
ABSTRACT:
Liquid epoxy resins are produced by contacting a dihydroxy phenol with an excess of epihalohydrin and an aqueous solution of an alkali metal hydroxide in a molar ratio of hydroxide to phenol not exceeding 2:1, recovering from the reaction products an epoxy resin having a content of hydrolyzable chlorine of from 1 to 6% by weight, contacting a solution of the resin in a hydrocarbon with an aqueous solution of an alkali metal hydroxide while maintaining an atomic ratio of alkali metal to hydrolyzable chlorine contained in the resin of from 1:1 to 1.17:1 and recovering from the reaction products a liquid epoxy resin having a content of hydrolyzable chlorine less than 0.02% by weight.
These epoxy resins of high purity are particularly useful as varnishes or coatings.
REFERENCES:
patent: 2841595 (1958-07-01), Pezzaglia
patent: 3069434 (1962-12-01), Spence et al.
Chemical Abstracts, vol. 60, (1964) 5704g.
Crespolini Giancarlo
Grazzini Giulio
Vargiu Silvio
Milestone Norma S.
Societa Italiana Resine S.I.R. S.p.A.
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