Process for the continuous preparation of diacetyl ethylene diam

Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing

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564216, C07C10204

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active

043249116

ABSTRACT:
A process for the continuous preparation of diacetyl ethylene diamine, w hich comprises allowing a mixture of ethylene diamine and acetic acid to react in a low-temperature zone at a temperature of about 80.degree. to 140.degree. C., completing the reaction of the mixture in a subsequent high-temperature zone of from about 140.degree. to 215.degree. C., discharging the diacetyl ethylene diamine obtained at the end of the high-temperature zone and stripping the reaction water in countercurrent flow by an inert gas at a point located between the low-temperature and the high-temperature zone.

REFERENCES:
patent: 615829 (1898-12-01), Fehrlin
patent: 3674851 (1972-07-01), Senoo et al.

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