Process for the brightening of sodium hydrogensulfate

Chemistry of inorganic compounds – Changing color characteristic of impurity

Reexamination Certificate

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C423S520000, C423S552000

Reexamination Certificate

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07067094

ABSTRACT:
The process for the brightening of continuously produced sodium hydrogensulfate obtained in the reaction of sodium chloride and concentrated sulfuric acid in molten sodium hydrogensulfate in a circulation reactor, wherein evolved hydrogen chloride and heating gases generated by an immersion burner are withdrawn at various sites and seed crystals are added for a faster conversion of initially formed metastable phases, is that from 0.01 to 0.05% by weight of aluminium oxide and/or from 0.5 to 1.5% by weight of magnesium oxide and/or magnesium sulfate and, optionally, additionally calcium sulfate are added as seed crystals.

REFERENCES:
patent: 1104913 (1914-07-01), Loeffler
patent: 1599996 (1926-09-01), Fritz
patent: 2861868 (1958-11-01), Stites, Jr. et al.
patent: 2893836 (1959-07-01), Davis et al.
patent: 3690825 (1972-09-01), Ott
patent: 3919401 (1975-11-01), Chay
patent: 28 10 693 (1979-09-01), None
patent: 110405 (1917-10-01), None
patent: 1 584 702 (1981-02-01), None
patent: 1 584 703 (1981-02-01), None
patent: 1 584 704 (1981-02-01), None
DERWENT Abstract accession No. 1977-67005Y, for DE 2619811, published Sep. 1977.

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