Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1974-11-27
1976-05-18
Patten, James A.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07D31300
Patent
active
039578259
ABSTRACT:
This invention provides a new synthesis for zearalanone and for related compounds having more or fewer carbon atoms in the non-aromatic ring than does zearalanone, which related compounds and zearalanone are represented by the formula ##SPC1##
Wherein X is an integer having a value from 2 to 6 inclusive and Y is an integer having a value from 2 to 8 inclusive. It also provides for new methods of making compounds useful in the synthesis of zearalanone and related compounds.
The new compounds useful as intermediates are 2,7-octadienoic acid; methyl 2,7-octadienoate; sodium ethyl 6-(4-pentenyl)-.beta.-dihydroresorcylate; ethyl 6-(4-pentenyl)-.beta.-dihydroresorcylate; sodium methyl 6-(4-pentenyl)-.beta.-dihydroresorcylate; methyl 6-(4-pentenyl)-.beta.-dihydroresorcylate; methyl 3-bromo-6-(4-pentenyl)-.beta.-dihydroresorcylate; methyl 6-(4-pentenyl)-.beta.-resorcylate; ethyl 6-(4-pentenyl)-.beta.-resorcylate; ethyl 6-(4-pentenyl)-.beta.-resorcylate dibenzyl ether; and 4-penten-2-yl 6-(4-pentenyl)-.beta.-resorcylate dibenzyl ether.
REFERENCES:
patent: 3631179 (1971-12-01), Urry
patent: 3810918 (1974-05-01), Urry et al.
patent: 3836544 (1974-09-01), Urry et al.
Mullenbach Guy Towns
Urry Wilbert Herbert
Commercial Solvents Corporation
Patten James A.
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