Organic compounds -- part of the class 532-570 series – Organic compounds – Amino nitrogen containing
Patent
1996-06-25
1998-02-03
Dees, Jose G.
Organic compounds -- part of the class 532-570 series
Organic compounds
Amino nitrogen containing
564305, 203 12, 203 13, C07C20936, B01D 300
Patent
active
057146349
ABSTRACT:
This invention relates to an improved process for storing and transporting toluenediamine, particularly for long term storage or storage in large containers, e.g., shipboard containers. The improvement in the process resides in substantially reducing the melting or freezing point of anhydrous toluenediamine obtained by the fractional distillation of a reaction product generated by the hydrogenation of dinitrotoluene. Such melting point reduction is accomplished by maintaining a water concentration in the toluenediamine in an amount of from 5 to 15% by weight under molten conditions for storage and transport. Preferably the level of water maintained in the toluenediamine is from about 7 to 10% by weight.
REFERENCES:
patent: 5449832 (1995-09-01), Carr et al.
Carr Richard Van Court
Casale Andrew James
Air Products and Chemicals Inc.
Badio Barbara
Brewer Russell L.
Dees Jos,e G.
Marsh William F.
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