Process for sintering reaction bonded silicon nitride

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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204 66, 501154, C04B 3558

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active

043517870

ABSTRACT:
Sintered silicon nitride articles are prepared from a silicon nitride compact by forming a silicon powder containing one or more sintering additives for silicon nitride into a compact having at density of at least 1.3 g/cm.sup.3, said additives being present in the powder in an amount such as to ensure an additive content of from 0.5 to 20 wt. % in the silicon nitride compact, nitriding the silicon compact by heating under nitrogen gas blanket at a temperature not exceeding 1500.degree. C., to convert said silicon into reaction bonded silicon nitride, and sintering the reaction bonded silicon nitride compact by heating in a nitrogen gas atmosphere at a temperature of at least 1500.degree. C.

REFERENCES:
patent: 3206318 (1965-09-01), Yamauchi et al.
patent: 4017319 (1977-04-01), Greskovich
patent: 4119690 (1978-10-01), Prochazka et al.
patent: 4127630 (1978-11-01), Washburn
Boyer et al., "A Mechanism for the Nitridation of Fe-Contaminated Silican", J. Materials Science, 13 (1938), p. 1637-1646.

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