Process for separation of vanillin by means of azeotropic distil

Distillation: processes – separatory – With disparate physical separation – Utilizing removing solid from liquid

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203 63, 568438, B01D 336

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active

055100066

ABSTRACT:
Vanillin is difficult to separate from second organic chemicals produced therewith such as parahydroxybenzaldehyde by conventional distillation or rectification because of the proximity of their boiling points. Vanillin can now be readily separated from such second organic chemicals by azeotropic distillation using as an effective azeotropic distillation agent, dibenzyl ether.

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Arnaud, et al., entitled "etude des gousses des vanille Madagascar/criteres analytiques de la recolte 1981", published by parfums, cosmetiques, aromes, No. 53, Oct.-Nov. 1983, pp. 99-101. Trnaslation into the English Language.
Derbesy, et al., entitled "contribution a letude des gousses de vanille/Criteres analytiques de differents lots de gousses Madagascar, Recolte 1980", published by parfums, cosmetiques, aromes, No. 43, Feb.-Mar. 1983, pp. 73-77. Translation into the English language.
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Buil, et al, parfums, cosmetiques, aromes, No. 52, Aug.-Sep. 1983, pp. 45-49, entitled: "Newly Identified Constituents in Concrete from Carnation Flowers".
Horsley, et al, entitled "Azeotropic Data", No. six of the "Advances in Chemistry Series"/American Chemical Society, published Jun. 1952, front cover page, pp. 1, 2, 218, 219 and 249 of interest.

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