Process for separating mixtures of substances of low volatility

Distillation: processes – separatory – Convective distillation with normally gaseous medium – e.g. – air

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203 58, 203 60, 203 62, 203 63, 203 67, 203 68, 203 69, 203 70, 203 75, 203 87, 203 96, 208348, 208356, 208357, 260419, 260428, 568869, B01D 336, C11C 110

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043459765

ABSTRACT:
The invention involves a process for substantially separating the components of mixtures of substances at least one of which is of low volatility while the other is of low or no volatility, the process using a compressed gas under supercritical conditions and an entrainer which increases the concentration of said mixture in the gaseous phase as well as the separation factor between the components to be separated. The process operates in two distillation zones the first of which substantially separates the components of low volatility in a process similar to a rectification process while the second distillation zone separates the top product of the first distillation zone from the gas with the aid of the entrainer which is condensed partially and in this state is passed in countercurrent to the gas carrying the separated component of low volatility.

REFERENCES:
patent: 1439685 (1922-12-01), Bodman
patent: 1965566 (1934-07-01), Beck et al.
patent: 2351249 (1944-06-01), Ziegler et al.
patent: 2838480 (1958-06-01), Swern et al.
patent: 3378467 (1968-04-01), Colton et al.
patent: 3806619 (1974-04-01), Zosel
patent: 3969196 (1976-07-01), Zosel

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