Process for separating low molecular weight compounds from polyc

Synthetic resins or natural rubbers -- part of the class 520 ser – Synthetic resins – Treating polymer containing material or treating a solid...

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528323, 528499, 528500, C08G 6946

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active

049636502

ABSTRACT:
A process for separating low molecular weight compounds from a crude polycaproamide melt comprises heat treating the melt in vacuo with superheated steam, in an extruder having a plurality of degassing zones, under precise conditions of temperature, pressure and configuration, such that the occurrence of side reactions and dehydration of the melt are substantially eliminated, the molecular weight of the polymer during the heat treatment in vacuo, during transport and subsequent processing remains substantially unchanged, a residual content of low molecular weight compounds of .ltoreq.1.8% is achieved, and the operating flexibility of the process is increased.

REFERENCES:
patent: 3361721 (1968-01-01), Markel et al.
patent: 4891420 (1990-01-01), Martin et al.

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