Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal
Patent
1980-06-13
1981-07-21
Roberts, Elbert L.
Chemistry of carbon compounds
Miscellaneous organic carbon compounds
C-metal
C07J 900
Patent
active
042798280
ABSTRACT:
A process for separating 3-hydroxy steroids from mixtures of lipids by combining a solution of the sterol-containing mixture in isopropanol or other similar alcoholic solvents with a slurry or solution of calcium dichloride in isopropanol or other similar alcoholic solvents. The complexed sterols are isolated by evaporating the alcoholic solvents, washing the residue with a hydrocarbon solvent and filtration. The sterols can be subsequently liberated from the complex by treatment with an aqueous/alcohol and isolated by filtration.
REFERENCES:
patent: 4057541 (1977-11-01), Weber et al.
patent: 4148810 (1979-04-01), Struve
Eastman Kodak Company
Reece III Daniel B.
Roberts Elbert L.
Tootle Clyde L.
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