Process for separating 2, 7-dimethylnaphthalene under pressure

Details Process for separating 2, 7-dimethylnaphthalene under pressure Process for separating 2, 7-dimethylnaphthalene under pressure

1991-09-09

1993-06-15

Pal, Asok

Chemistry of hydrocarbon compounds

Purification, separation, or recovery

By cooling of liquid to obtain solid, e.g., crystallization,...

C07C 714

Patent

active

052200981

ABSTRACT:
The present invention relates to a process for separating 2,7-DMN, characterized in that a mixture containing at least 50% by weight of 2,7-DMN and the other DMN isomers obtained by preliminarily concentrating a fraction in the range of 250.degree.-270.degree. C. of catalytically cracked petroleum oil is preliminarily adjusted to a temperature of 60.degree.-90.degree. C. to form a slurry containing the crystal of 2,7-DMN, which is placed in a tightly sealed pressure vessel, adiabatically pressurized to the range of 500-2,500 kgf/cm.sup.2 and solidified to form a state of co-existing of solid and liquid phases, liquid is then discharged under pressure from the solid-liquid co-existing system, the solid remaining in the vessel is pressed to discharge the liquid remaining between the solid particles, which are integrated to give 2,7-DMN having a purity of 98% by weight or more.

REFERENCES:
patent: 3202726 (1965-08-01), Malmberg et al.
patent: 3590091 (1971-06-01), Skarada et al.

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