Process for selenium purification

Chemistry of inorganic compounds – Selenium or tellurium or compound thereof – Elemental selenium or tellurium

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423508, 75121, C01B 1902

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active

045488002

ABSTRACT:
This invention is generally directed to an improved process for the preparation of selenium of high purity which comprises reacting selenious acid, selenium oxides, or mixtures thereof, with an alcohol, and subjecting the resulting selenium ester, subsequent to purification to a reduction reaction.

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Zingaro, Ralph A. & Cooper, W. Charles, Selenium, Van Nostrand Reinhold Co., 1974, pp. 62-63.
Paul, R. C. et al., "Preparation of Dialkyl Selenites Indian", Journal of Chemistry, vol. 13, #3, Mar. 1975, pp. 292-294.
Bunton, C. A. & Hendy N. B., J. Chem. Soc. 1963 3137, "Tracer Studies in Ester Hydrolysis Part XIII."

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