Process for reproducibly preparing titanium subhydride

Details Process for reproducibly preparing titanium subhydride Process for reproducibly preparing titanium subhydride

1980-05-30

1982-01-05

Carter, Herbert T.

Explosive and thermic compositions or charges

Processes of making

149 77, 149 87, 423645, C06B 4300, C01G 2300

Patent

active

043092306

ABSTRACT:
Titanium subhydride is produced in a reactor by heating a selected amount of finely divided titanium compound at a selected temperature for a selected period of time under dynamic vacuum conditions. Hydrogen is removed substantially uniformly from each powder grain and there is produced a subhydride of substantially uniform titanium-hydrogen composition. Selection of the amount, temperature and time produces a subhydride of selected titanium-hydrogen composition.

REFERENCES:
patent: 3180711 (1965-04-01), Aconsky
patent: 3376107 (1968-04-01), Oka
Lieberman, "Chemical Abstracts", vol. 90, 1979, #124081(e).
Gibb et al., "Journal of American Chemical Society", vol. 72, 1950, pp. 5365-5369.

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