Process for removing insoluable N-vinyl amide polymer from equip

Cleaning and liquid contact with solids – Processes – Hollow work – internal surface treatment

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134 2219, 134 38, 134 42, 510201, 510202, 510206, 510212, B08B 308, B08B 900, B08B 908, C23D 1700

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057699593

ABSTRACT:
Insoluble polymer formed during the distillation of N-vinylformamide is removed by contacting the insoluble polymer with an aqueous weakly basis solution in a closed system at elevated temperature. Polymer (up to 50 wt % polymer gel or 5.5 wt % dry polymer in reaction mixture) is treated with an aqueous solution of an amine, alkanolamine or weak inorganic base having a concentration of at least 1 molar. Solvents like alcohols, glycol ethers or amides may be added as a cosolvent in an amount of from 0 to about 85% by weight.

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James E. Banks,"A Programmed Introduction to Organic Chemistry" Naming Organic Compounds, Second Edition.
W.B Saunders Company, 1976, pp. 216-220.

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