Process for removal of basic materials

Tobacco – Tobacco treatment – Extraction of component – other than moisture – by contact...

Patent

Rate now

  [ 0.00 ] – not rated yet Voters 0   Comments 0

Details

131298, 131352, 131356, 131310, 426427, 426428, 4236585, A24B 1524, A24B 1526

Patent

active

050185403

ABSTRACT:
A process is provided for the selective removal of basic materials from plant products, in particular, for removing nicotine from tobacco without materially affecting the content of the other components of the tobacco. Tobacco is traversed with a solvent at high pressure and in a physical state which is either a liquid at a pressure of from about 500-300 atmospheres or a supercritical fluid wherein nicotine and the other components dissolve in the solvent. As the single means of removing substances from the solvent, the solvent is then passed through an acid-containing trap where the solvent is essentially freed of nicotine. The solvent, depleted of nicotine and enriched in the other components, is then recycled to the tobacco to reextract nicotine. In addition, the tobacco may be pretreated with a chemical base which does not substantially react with the tobacco components under ambient conditions and which are not necessarily affected by the process conditions but are nonetheless effective in increasing the amount of nicotine which can be extracted by the process of this invention. Pretreatment of the tobacco with a chemical base neutralizes nicotine salts and permits the extraction process to be carried out under milder conditions.

REFERENCES:
patent: 283622 (1882-08-01), Liebrich et al.
patent: 678362 (1901-07-01), Froehling
patent: 802487 (1905-10-01), Wimmer
patent: 896124 (1908-08-01), Lindenberger et al.
patent: 1196184 (1916-08-01), Villiers-Stuart
patent: 1294310 (1919-02-01), Sayre et al.
patent: 1577768 (1926-03-01), Smith
patent: 1671259 (1928-05-01), Schloesing
patent: 1813833 (1931-07-01), Andrews
patent: 1823554 (1931-09-01), Mewborne
patent: 1859379 (1932-05-01), Chesley
patent: 1984445 (1934-12-01), Wagner
patent: 2048624 (1936-07-01), Roselius
patent: 2128043 (1938-08-01), Garner
patent: 2162738 (1939-06-01), McCoy
patent: 2227863 (1941-01-01), Rhodes
patent: 2286639 (1942-06-01), Ott
patent: 2582075 (1952-01-01), Severi
patent: 2805667 (1957-09-01), von Bethmann
patent: 2822306 (1958-02-01), Thienemann et al.
patent: 3046997 (1962-07-01), Hind
patent: 3096773 (1963-07-01), Neukomm et al.
patent: 3110315 (1963-11-01), Lendvai
patent: 3139435 (1964-06-01), Staley et al.
patent: 3151118 (1964-09-01), Moser
patent: 3390685 (1968-07-01), von Bethmann et al.
patent: 3396735 (1968-08-01), von Bethmann et al.
patent: 3424171 (1969-01-01), Rooker
patent: 3482328 (1969-12-01), Larkham
patent: 3612066 (1971-10-01), Jones et al.
patent: 3742962 (1973-07-01), Brochot
patent: 3771533 (1973-11-01), Armstrong et al.
patent: 3821960 (1974-07-01), Egri
patent: 3874392 (1975-04-01), DeBrunn et al.
patent: 4068671 (1978-01-01), Casey
patent: 4123592 (1978-10-01), Rainer et al.
patent: 4153063 (1979-05-01), Roselius et al.
patent: 4215706 (1980-08-01), Larson et al.
patent: 4243056 (1981-01-01), de la Burde
patent: 4248252 (1981-02-01), Lendvay et al.
patent: 4506682 (1985-03-01), Muller
patent: 4548755 (1985-10-01), Stahl et al.
patent: 4561452 (1985-12-01), Gahrs
patent: 4607646 (1986-08-01), Lill et al.
patent: 4628947 (1986-12-01), Driscoll et al.
patent: 4677994 (1987-07-01), Denier et al.
patent: 4700722 (1987-10-01), Korte et al.
patent: 4714617 (1987-12-01), Gahrs
patent: 4727889 (1988-03-01), Niven, Jr. et al.
L. N. Luganskaja, E. B. Kransnokutskaj and L. B. Jasinskaja, "The Use of Tobacco Dust Extract for Aromatizing Purposes", Tabak, SSSR, 1, pp. 30-33 (1967).
W. R. Harvey, H. M. Stahrand, W. C. Smith, "Automated Determination of Reducing Sugars and Nicotine Alkaloids on the Same Extract of Tobacco", Tobacco Science, 168, pp. 48-50 (1969).
L. N. Luganskaja, "On the Aromatization of Tobacco", Trav. Inst. Rech., Sci., Kransnodor, 3, pp. 199-205 (1967) as cited in Tobacco Abstracts, 12, pp. 394-395 (1968).
P. Hubert and O. G. Vitzhthum, "Fluid Extraction of Hops, Spices and Tobacco with Supercritical Gases", Angewandte Chemie, Int. Ed. Engl., 17, pp. 710-715 (1978).
D. F. Williams, "Extraction with Supercritical Gases", Review Article No. 5, Chemical Engineering Science, 36, pp. 1769-1788, 1781 (1981).

LandOfFree

Say what you really think

Search LandOfFree.com for the USA inventors and patents. Rate them and share your experience with other people.

Rating

Process for removal of basic materials does not yet have a rating. At this time, there are no reviews or comments for this patent.

If you have personal experience with Process for removal of basic materials, we encourage you to share that experience with our LandOfFree.com community. Your opinion is very important and Process for removal of basic materials will most certainly appreciate the feedback.

Rate now

     

Profile ID: LFUS-PAI-O-28310

  Search
All data on this website is collected from public sources. Our data reflects the most accurate information available at the time of publication.