Process for reducing organic compounds with calcium, amine, and

Details Process for reducing organic compounds with calcium, amine, and Process for reducing organic compounds with calcium, amine, and

1984-08-23

1985-08-06

Gantz, D. E.

Organic compounds -- part of the class 532-570 series

Organic compounds

Oxygen containing

568631, 585266, 585267, 585271, C07C 510

Patent

active

045337608

ABSTRACT:
Olefins are produced by contacting an organic compound having at least one benzene ring with calcium metal, ethylenediamine, a low molecular weight aliphatic alcohol, and optionally a low molecular weight aliphatic primary amine, and/or an inert, abrasive particulate substance. The reduction is conducted at temperatures ranging from about -10.degree. C. to about 30.degree. C. or somewhat higher. Substantially all of the organic compounds are converted to corresponding cyclic olefins, primarily diolefins.

REFERENCES:
patent: 3278618 (1966-10-01), Amagasa et al.
Benkeser et al., J. Org. Chem., 44, 3737-39, (1979).
Benkeser et al., J. Org. Chem., 48, 2796-2802, (1983).
Benkeser et al., Synth. Commun., 13, 1103-16, (1983).
Benkeser et al., Tetrahedron Lett., 25, 2089-92, (1984).

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