Process for recovering phosphate ester type hydraulic fluids fro

Distillation: processes – separatory – With chemical reaction – Including step of adding catalyst or reacting material

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203 80, 203 89, 203 91, 203 72, 203 39, 72 42, 252 325, 260990, B01D 122, B01D 328, C10M 144

Patent

active

042279720

ABSTRACT:
Disclosed herein is a process for recovering a phosphate ester type hydraulic fluid from a waste liquid containing water, organic solvents and other impurities, such as polychlorinated biphenyls (PCB). After filtering to remove particulate matter, a heavy fraction separated from the waste liquid and consisting primarily of the hydraulic fluid is first subjected to a distillation step. A substantial portion of the PCB is removed as overhead from the distillation step and the bottoms containing the hydraulic fluid is subsequently evaporated, preferably in a thin film evaporator. The overhead from the evaporation step is condensed to recover the hydraulic fluid.

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patent: 3679550 (1972-07-01), Orwoll
patent: 3945891 (1976-03-01), Aal et al.
patent: 4016048 (1977-04-01), Gerhmann et al.
patent: 4092378 (1978-05-01), Damiani et al.
patent: 4138346 (1979-02-01), Nassry et al.

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