Process for recovering of dialkylaluminum halide from mixtures c

Chemistry of carbon compounds – Miscellaneous organic carbon compounds – C-metal

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2604299, C07F 506

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active

039460584

ABSTRACT:
A process is disclosed for the recovery of dialkylaluminum halides from a mixture containing dialkylaluminum halides and soluble zinc containing compounds by heating the mixture to pyrolyze the zinc compounds down to acceptable levels and subsequently distilling the alkylaluminum halide from the heated mixture.

REFERENCES:
patent: 2996529 (1961-08-01), Bos
patent: 3072697 (1963-01-01), Jenkner
patent: 3074986 (1963-01-01), Kaster et al.
patent: 3124604 (1964-03-01), Huther
patent: 3475475 (1969-10-01), Eidt
Nesmeyanvo et al., Methods of Elements-Organic Chem. North-Holland Pub. Co. Amsterdam, Vol. 1, p. 400 (1967).
Rochow et al., The Chemistry of Organometallic Compounds, John Wiley & Sons N.Y. p. 105 (1957).

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