Process for purifying unsaturated carboxylic acids using distill

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

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562600, C07B 3504, C07C 5142, C07C 5100

Patent

active

055234801

ABSTRACT:
A process for the preparation of an .alpha.,.beta.-unsaturated C.sub.3 -C.sub.6 carboxylic acid of greater than 98% purity, which combines fractional distillation and melt crystallization procedures.

REFERENCES:
patent: Re32241 (1986-09-01), Saxer
patent: 4671857 (1987-06-01), Johnson
patent: 4780568 (1988-10-01), Pascoe
N. P. Wynn, Separate Organics by Melt Crystallization, Chem. Eng. Progress, 88(3), 55-57, (1992).
N. P. Wynn, Chem. Eng. Progress, 88(3), 52-60 (1992).
Khim. Prom. (2) 106-109 (1979).
Khim. Prom. (8) 486-488 (1984).

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