Process for purification of DMT by film crystallization

Single-crystal – oriented-crystal – and epitaxy growth processes; – Processes of growth from liquid or supercritical state – Having growth from a solution comprising a solvent which is...

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117 73, 117925, 117927, 23295R, C30B 2954

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active

055423728

ABSTRACT:
This invention relates to a single crystallization process for purification of dimethyl terephtalate (DMT) by film crystallization, including pumping the raw DMT into a film crystallizer and reducing its temperature to form DMT crystalline on the walls of the crystallizing pipes in the crystallizer, and then heating the crystallizing pipes and collecting the melt at 140.degree.-145.degree. C. The product DMT is thus obtained.

REFERENCES:
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patent: 3576842 (1971-04-01), Kimura et al.
patent: 3621664 (1971-11-01), Saxer
patent: 3686276 (1972-08-01), Slockett
patent: 4683034 (1987-07-01), Bader et al.
patent: 5116518 (1992-05-01), Bachmann et al.
patent: 5338882 (1994-08-01), Korte

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