Process for purification of crude p-hydroxymethylbenzoic acid

Organic compounds -- part of the class 532-570 series – Organic compounds – Carboxylic acids and salts thereof

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C07C 6500

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048125946

ABSTRACT:
Aqueous solutions of crude p-hydroxymethylbenzoic acid are purified to relatively low levels of 4-carboxybenzaldehyde by hydrogenation in the presence of a nickel on kieselguhr catalyst. 4-carboxybenzaldehyde is hydrogenated to p-hydroxymethylbenzoic acid. Toluic acid production is minimal.

REFERENCES:
patent: 4721808 (1988-01-01), Lillwitz

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