Process for production of essentially chloride-free calcium...

Organic compounds -- part of the class 532-570 series – Organic compounds – Sulfonic acids or salts thereof

Reexamination Certificate

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Reexamination Certificate

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07094922

ABSTRACT:
The invention relates to a process for the preparation of a low-base number calcium sulfonate that is essentially chloride free. The process involves preparing a sulfonic acid solution by adding a solvent to a sulfonic acid, optionally removing dissolved or entrained SO2or SO3, mixing the solution with a specific amount of water and calcium hydroxide, heating the mixture, separating out excess calcium hydroxide from the mixture, removing the solvent and recovering the calcium sulfonate product in oil.

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