Distillation: processes – separatory – Plural distillations performed on same material – One a distillation under positive pressure or vacuum
Patent
1996-07-29
1998-11-17
Manoharan, Virginia
Distillation: processes, separatory
Plural distillations performed on same material
One a distillation under positive pressure or vacuum
203 6, 203 12, 203 79, 203 80, 203 92, 203 93, 203 94, 203 96, 203 97, 203 98, 203 99, 203DIG19, 423387, B01D 338, C01B 2114
Patent
active
058371079
ABSTRACT:
An aqueous solution of free hydroxylamine is prepared by a process in which the solution obtained by treating a hydroxylammonium salt with a base is separated into an aqueous hydroxylamine solution and a salt fraction by treatment with water or steam at .ltoreq.80.degree.0 C. The novel process can be carried out in a simple and gentle manner and on a large industrial scale. Owing to the low thermal load, the low concentration of hydroxylamine and the short residence time in the process, the risk of decomposition is minimized.
REFERENCES:
patent: 4956168 (1990-09-01), Wagaman
patent: 5266290 (1993-11-01), Levinthal et al.
patent: 5472679 (1995-12-01), Levinthal et al.
patent: 5510097 (1996-04-01), Cawlfield et al.
Friederang Albrecht Wilhelm
Leutner Bernd
Schneider Hans-Michael
Watzenberger Otto
BASF - Aktiengesellschaft
Manoharan Virginia
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