Chemistry of inorganic compounds – Boron or compound thereof – Oxygen containing
Patent
1987-11-10
1989-03-28
McFarlane, Anthony
Chemistry of inorganic compounds
Boron or compound thereof
Oxygen containing
423279, 423283, 423286, 423371, 423419P, 423419R, 423420, 423593, 423594, 423598, 423599, 423608, 423600, 23293R, 23295R, 23302A, C01B 3500, C01C 126, C01G 2500
Patent
active
048162396
ABSTRACT:
A process for producing acidic boratozirconium chloride sols which comprises: reacting a zirconium compound with a boron compound in molar ratios of B/Zr of 0.3-1.2 together with a compound of a metal M other than boron, the metal M being selected from the group consisting of divalent, trivalent, tetravalent and pentavalent metals in molar ratios of M/Zr of about 0.01-1 in water in the presence of chloride ions in molar ratios of Cl/Zr of not less than about 1.
The acidic boratozirconium chloride sol may be converted to basic boratozirconium sols by reacting the acidic sol with a basic carbonate compound such as ammonium carbonate.
The sols, either acidic or basic, are readily gelled by contact with a dehydration solvent such as methanol or acetone.
The gel is calcined at relatively low temperatures to provide zirconia which is either very pure or stabilized in varied degrees.
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Matsuda Hideaki
Onaka Hiroshi
Wada Takeo
McFarlane Anthony
Takeda Chemical Industries Ltd.
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