Process for producing tris (N-methylamino) methylsilane

Details Process for producing tris (N-methylamino) methylsilane Process for producing tris (N-methylamino) methylsilane

1983-05-09

1984-10-02

Shaver, Paul F.

Organic compounds -- part of the class 532-570 series

Organic compounds

Silicon containing

C07F 708, C07F 710

Patent

active

044749759

ABSTRACT:
A method of producing tris (N-methylamine) methylsilane, including the steps of forming and cooling a liquid solution of methylamine in an inert solvent and under an inert atmosphere at a temperature of about -30.degree. C. and slowly adding a quantity of methyltrichlorosilane while maintaining said temperature. The reaction mixture is then heated for about 60 minutes at a temperature of about 40.degree. C., followed by filtering the solid portion from the liquid portion. The liquid is distilled to remove the solvent, resulting in a high yield of tris (N-methylamine) methylsilane.

REFERENCES:
patent: 2429883 (1947-10-01), Johannson
patent: 2579417 (1951-12-01), Cheronis
patent: 2807635 (1957-09-01), Breederveld et al.
patent: 3481964 (1969-12-01), Ismail et al.

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