Organic compounds -- part of the class 532-570 series – Organic compounds – Heterocyclic carbon compounds containing a hetero ring...
Patent
1990-06-22
1994-08-30
Shah, Mukund J.
Organic compounds -- part of the class 532-570 series
Organic compounds
Heterocyclic carbon compounds containing a hetero ring...
549248, 562412, 562413, 562414, C07D30783
Patent
active
053429680
ABSTRACT:
A process for making relatively high purity eulfonylbis(phthalic anhydride) is provided. 3,3',4,4'-tetramethyl diphenyl sulfone is catalytically oxidized in a solvent under liquid phase elevated temperature and pressure conditions. The catalyst is constituted by cobalt, manganese, zirconium, and bromine. Sulfonylbis(phthalic) acid is recovered by crystallization and is then heated to produce the anhydride. Preferably, the acid is purified prior to dehydration.
REFERENCES:
patent: 3022320 (1962-02-01), Woodbury et al.
patent: 3920735 (1975-11-01), Wampfler et al.
Brugge Stephen P.
Holzhauer Juergen K.
Wolff Thomas E.
Amoco Corporation
Gupta Y. N.
Henes James R.
Nemo Thomas E.
Oliver Wallace L.
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