Process for producing stable, low odor S,S,S-tributylphosphorotr

Organic compounds -- part of the class 532-570 series – Organic compounds – Phosphorus esters

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558 71, C07F 902, C07F 9165

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active

051891956

ABSTRACT:
Stable S,S,S-tributylphosphorotrithioate having reduced levels of the odorous by-product dibutyl disulfide is produced by adding a caustic solution having a concentration of less than 10% to crude S,S,S-tributylphosphorotrithioate until the pH remains constant. In a preferred embodiment, a solution of sodium hydroxide having a concentration of less than 10% is used in an amount such that at least 0.1 mole of sodium hydroxide is present for each mole of crude S,S,S-tributylphosphortrithioate.

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