Chemistry of inorganic compounds – Treating mixture to obtain metal containing compound – Alkali metal
Patent
1977-10-25
1981-09-22
Vertiz, O. R.
Chemistry of inorganic compounds
Treating mixture to obtain metal containing compound
Alkali metal
423190, 423422, 423426, 423427, C01D 700, C01D 737
Patent
active
042910021
ABSTRACT:
A process for the production of sodium carbonate wherein sodium bicarbonate is recovered from a brine containing sodium carbonate by carbonation of the brine under controlled conditions. The sodium bicarbonate is crystallized from the carbonated brine in a multi-stage carbonating, cooling and crystallization process after which it is filtered to produce wet cake. The wet cake is subjected to predrying to provide a predried wet cake of a specified free moisture content and mixed with recycle light ash to provide a dryer feed of specified moisture content to alleviate problems of product fouling or plugging of the dryer. The light ash from the dryer then is bleached and subjected to recrystallization, screening, centrifuging and drying to provide a dried sodium carbonate possessing, after evaporation of the water of hydration and free moisture, less than 0.10 percent moisture and chemical and physical properties meeting commercial dense ash specifications.
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Manufacture of Soda by Te-Pang Hou, Ph.D., Reinhold Publishing Corporation (1942), pp. 173-179.
Arnold Donald S.
Coe Merlin D.
Fairchild James L.
Nichols Donald A.
Addison William G.
Kerr-McGee Chemical Corporation
Langel Wayne A.
Vertiz O. R.
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