Process for producing Si.sub.3 N.sub.4 base articles by the cold

Plastic and nonmetallic article shaping or treating: processes – Including step of generating heat by friction

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51307, 106 734, 264 65, C04B 3558

Patent

active

042809738

ABSTRACT:
A method of making Si.sub.3 N.sub.4 based cutting tools (and the resulting product) is disclosed. A mixture is formed of three powders: a first powder of at least 75% crystalline Si.sub.3 N.sub.4, a second powder selected from the group Y.sub.2 O.sub.3, MgO, CeO.sub.2 and ZrO.sub.2, and a third powder selected from the group consisting of Al.sub.2 O.sub.3, WC, Wsi.sub.2, W and TiC. The mixture is cold pressed to a density of 50-70% of theoretical and then sintered to full density without the application of pressure.

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Giachello et al., "Sintering of Silicon Hatride in a Powder Bed", J. Mat. Sci., 14 (1979) 2825-2830.

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