Process for producing phytosterols by saponification in an...

Organic compounds -- part of the class 532-570 series – Organic compounds – Cyclopentanohydrophenanthrene ring system containing

Reexamination Certificate

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Reexamination Certificate

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10129279

ABSTRACT:
The present invention provides a method of obtaining highly pure phytosterols practically and efficiently from crude phytosterol compositions derived from vegetable fats and oils. That is, the present invention provides a method of saponifying fatty esters contained in crude phytosterol compositions with an alkali in a mixed solvent of an lower alcohol and water, as well as a process for producing phytosterols, which comprises, after this saponifying method, cooling the reaction solution to precipitate crystals of phytosterols, and separating the obtained crystals.

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Nekrasova et al., “Separation of phytosterol from aqueous alcohol solutions of saponified pitch by crystallization using the LTA method.” Izv. Vys. Uch. Zav., Lesnoi Zhurnal, vol. 17(6), pp. 105-108 (English Abstract Only).
Database Paperchem2 ′Online! Institute of Paper Science and Technology (IPST); 1975 Nekrasova, V.B. et al.: “Separation of Phytosterol From Aqueous Alcohol Solutions of Saponified Pitch by Crystallization Using the LTA Method” retrieved from STN Database accession No. 2764 XP002161740 abstract & Izv. Vuz. Lesnoi Zh., (1974) vol. 17, No. 6, pp. 105-108, ′Russ.!., Abstract Only.
Database Biosis ′Online! Biosciences Information Service, Philadelphia, PA, US; 1993 Biedermann Maurus et al: “Transesterification and on-line LC-GC for determining the sum of free and esterified sterols in edible oils and fats.” Database accession No. PREV199396027425 XP002161742 abstract & FETT Wissenschaft Technologie, vol. 95, No. 4, 1993, pp. 127-133, ISSN: 0931-5985, Abstract Only.

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